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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2014  >  32(6): 448-452

GAO Yanxia, SU Juan, JIN Huizi. Study on HPLC fingerprint of Ginseng Radix et Rhizoma Rubra[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(3): 249-251,254. doi: 10.3969/j.issn.1006-0111.2016.03.014
Citation: LI Ling, Lü Lei, DONG Xin, LV Diya, LOU Ziyang. Rapid identification of chemical components in Artemisiae argyi folium by RRLC-TOFMS[J]. Journal of Pharmaceutical Practice and Service, 2014, 32(6): 448-452. doi: 10.3969/j.issn.1006-0111.2014.06.012
shu

Rapid identification of chemical components in Artemisiae argyi folium by RRLC-TOFMS

doi: 10.3969/j.issn.1006-0111.2014.06.012
  • 1.

    Pharmaceutical Analysis Center, School of Pharmacy, Second Military Medical University, Shanghai 200433, China

  • 2.

    Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital affiliated to Second Military Medical University, Shanghai 200438, China

  • Received Date: 2013-06-09
  • Rev Recd Date: 2013-11-13
  • Objective To identify the chemical components in Artemisiae argyi folium by rapid resolution liquid chromatography-time of flight mass spectrometry (RRLC-TOFMS). Methods The separation was performed on an Agilent Eclipse C18 column (2.1 mmü100 mm,1.8 μm ). The mobile phase consisted of acetonitrile (A) and 0.1% formic acid (B) were in gradient elution.The flowing rate was 0.35 ml/min, the injection volume was 1 μl and the temperature of column was 40℃. Time of flight mass spectrometer (TOFMS) with electro spray ion source (ESI) was applied to qualitative analysis under the positive ion mode,and mass scan range was m/z 100-1 500. Results 31 chemical compounds in Artemisiae argyi folium were identified unequivocally. Conclusion A rapid and efficient RRLC-TOFMS approach for identifying the chemical constituents of Artemisiae argyi folium had been successfully established,which paved a way for quality control and further in vivo studies of Artemisiae argyi folium.
  • [1] 国家药典委员会.中华人民共和国药典一部[S].北京:中国医药科技出版社,2010:82.
    [2] 周 峰,秦路平,连佳芳,等.艾叶的化学成分、生物活性和植物资源[J].天然药物,2002,18(2):96-98.
    [3] 梅全喜,高玉桥.艾叶化学及药理研究进展[J].中成药,2006,28(7):1030-1032.
    [4] 兰美兵,余永莉,李啸红.贵州产艾叶挥发油的化学成分分析[J].药物分析杂志,2009,29(8):1305-1308.
    [5] 钱 伟,韩 乐,刘训红,等.野艾叶与艾叶的挥发性成分HSGC-MS比较分析[J].中华中医药学刊,2010,28(7):766-768.
    [6] 戴小军,刘延庆,梅全喜. 蒿属药用植物药理活性研究进展[J].中药材,2005,28(3):243-247.
    [7] 吕 磊,张 海,赵 亮,等.RRLC-TOF/MS快速鉴别中药淫羊藿中43种化学成分[J].第二军医大学学报,2011,32(3):941-946.
    [8] 赵 亮,田文君,吕 磊.HPLC-TOF/MS对中药扶正平消胶囊化学成分的鉴别[J].第二军医大学学报,2012,33(7):770-779.
    [9] 王锦军,黄兆文,李瑶瑶.艾叶化学成分的研究[J].药学服务与研究,2008,8(6):465-466.
    [10] Tian F,Liu L,Dou DQ,et al.Chemical comparison of Artemisia borealis and three Chinese Artemisia plant[J].J Chin Pharm Sci,2007(16):27-32.
    [11] 杨晓军,涂院海.陕西艾叶化学成分的研究[J].天然产物研究与开发,2007,(19):402-403.
    [12] Lopes-Lutz D,Alviano DS,Alviano CS,et al.Screening of chemical composition, antimicrobial and antioxidant activities of Artemisia essential oils[J].Phytochemistry,2008(69):1732-1738.
    [13] 吉 双,张予川,亓云鹏.艾叶的化学成分[J].沈阳药科大学学报,2009,26(8):617-619.
    [14] Miron TL,Plaza M,Bahrim G,et al.Chemical composition of bioactive pressurized extracts of Romanian aromatic plants[J].J Chromatogr A,2011,1218(30):4918-4927.
    [15] 高淑丽,刘丽华,张 阳,等.LC-MS/MS法同时测定连翘叶中4种成分的含量[J].中国药房,2013,24(11):1026-1028.
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    Created with Highcharts 5.0.7Chart context menuAccess Class DistributionFULLTEXT: 89.0 %FULLTEXT: 89.0 %META: 7.6 %META: 7.6 %PDF: 3.4 %PDF: 3.4 %FULLTEXTMETAPDFHighcharts.com
    Created with Highcharts 5.0.7Chart context menuAccess Area Distribution其他: 20.2 %其他: 20.2 %China: 1.4 %China: 1.4 %India: 0.4 %India: 0.4 %上海: 2.8 %上海: 2.8 %东莞: 0.4 %东莞: 0.4 %临汾: 0.4 %临汾: 0.4 %乌鲁木齐: 0.2 %乌鲁木齐: 0.2 %信阳: 0.2 %信阳: 0.2 %北京: 11.9 %北京: 11.9 %南京: 0.2 %南京: 0.2 %南宁: 0.2 %南宁: 0.2 %南昌: 0.5 %南昌: 0.5 %南通: 0.2 %南通: 0.2 %台湾省: 0.2 %台湾省: 0.2 %合肥: 0.2 %合肥: 0.2 %咸阳: 0.5 %咸阳: 0.5 %唐山: 1.2 %唐山: 1.2 %大连: 0.9 %大连: 0.9 %天津: 0.4 %天津: 0.4 %孝感: 0.2 %孝感: 0.2 %安顺: 0.2 %安顺: 0.2 %广州: 0.9 %广州: 0.9 %张家口: 0.7 %张家口: 0.7 %惠州: 0.2 %惠州: 0.2 %成都: 0.7 %成都: 0.7 %无锡: 0.2 %无锡: 0.2 %昆明: 0.2 %昆明: 0.2 %杭州: 0.4 %杭州: 0.4 %梧州: 0.2 %梧州: 0.2 %武汉: 0.5 %武汉: 0.5 %洛阳: 0.2 %洛阳: 0.2 %济南: 0.2 %济南: 0.2 %深圳: 0.7 %深圳: 0.7 %漳州: 0.2 %漳州: 0.2 %濮阳: 0.2 %濮阳: 0.2 %盐城: 0.4 %盐城: 0.4 %石家庄: 0.5 %石家庄: 0.5 %聊城: 0.2 %聊城: 0.2 %芒廷维尤: 26.2 %芒廷维尤: 26.2 %芝加哥: 0.2 %芝加哥: 0.2 %苏州: 0.5 %苏州: 0.5 %菏泽: 0.2 %菏泽: 0.2 %西宁: 20.5 %西宁: 20.5 %西安: 0.2 %西安: 0.2 %赤峰: 0.4 %赤峰: 0.4 %运城: 0.9 %运城: 0.9 %郑州: 0.2 %郑州: 0.2 %长沙: 0.4 %长沙: 0.4 %长治: 0.5 %长治: 0.5 %黄冈: 0.9 %黄冈: 0.9 %黄冈市麻城: 0.2 %黄冈市麻城: 0.2 %其他ChinaIndia上海东莞临汾乌鲁木齐信阳北京南京南宁南昌南通台湾省合肥咸阳唐山大连天津孝感安顺广州张家口惠州成都无锡昆明杭州梧州武汉洛阳济南深圳漳州濮阳盐城石家庄聊城芒廷维尤芝加哥苏州菏泽西宁西安赤峰运城郑州长沙长治黄冈黄冈市麻城Highcharts.com
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Rapid identification of chemical components in Artemisiae argyi folium by RRLC-TOFMS

doi: 10.3969/j.issn.1006-0111.2014.06.012
  • 1. Pharmaceutical Analysis Center, School of Pharmacy, Second Military Medical University, Shanghai 200433, China
  • 2. Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital affiliated to Second Military Medical University, Shanghai 200438, China
  • Received Date: 2013-06-09
  • Rev Recd Date: 2013-11-13

Abstract: Objective To identify the chemical components in Artemisiae argyi folium by rapid resolution liquid chromatography-time of flight mass spectrometry (RRLC-TOFMS). Methods The separation was performed on an Agilent Eclipse C18 column (2.1 mmü100 mm,1.8 μm ). The mobile phase consisted of acetonitrile (A) and 0.1% formic acid (B) were in gradient elution.The flowing rate was 0.35 ml/min, the injection volume was 1 μl and the temperature of column was 40℃. Time of flight mass spectrometer (TOFMS) with electro spray ion source (ESI) was applied to qualitative analysis under the positive ion mode,and mass scan range was m/z 100-1 500. Results 31 chemical compounds in Artemisiae argyi folium were identified unequivocally. Conclusion A rapid and efficient RRLC-TOFMS approach for identifying the chemical constituents of Artemisiae argyi folium had been successfully established,which paved a way for quality control and further in vivo studies of Artemisiae argyi folium.

GAO Yanxia, SU Juan, JIN Huizi. Study on HPLC fingerprint of Ginseng Radix et Rhizoma Rubra[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(3): 249-251,254. doi: 10.3969/j.issn.1006-0111.2016.03.014
Citation: LI Ling, Lü Lei, DONG Xin, LV Diya, LOU Ziyang. Rapid identification of chemical components in Artemisiae argyi folium by RRLC-TOFMS[J]. Journal of Pharmaceutical Practice and Service, 2014, 32(6): 448-452. doi: 10.3969/j.issn.1006-0111.2014.06.012
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