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HUANG Xiong-wei, Gu Li-hong. Analyzing the content of rivanol in preparation with back-dropping method[J]. Journal of Pharmaceutical Practice and Service, 2001, (3): 170-171.
Citation:
CAO Qin, CHEN Jian-tao. Studies on the chemical constituents of Cirsium segestum[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(4): 271-273.
Studies on the chemical constituents of Cirsium segestum
No.8690 Hospital of People's Armed Police,Yixing 214206,China
2.
Shanghai First biochemical &Pharmaceutical company LTD.,Shanghai 200240,China
Received Date: 2010-05-07
Rev Recd Date:
2010-06-24
Abstract
Objective To study the chemical constituents of Cirsium segestum. Methods Multi-chromatographic Methods including Silica gel column chromatography and Sephadex LH-20 gel permeation were employed for the isolation and purification.The structures were identified on the basis of chemical evidence and spectral data. Results Five compounds were isolated and identified as Caffeic acid(Ⅰ),Chlorogenic acid(Ⅱ),Baicalin(Ⅲ),stigmasterol 3-O-glucopyranoside(Ⅳ),5,8,4'-trihydroxy-7-O-β-D-glucopyranoside(Ⅴ). Conclusion compounds Ⅳ and Ⅴwere isolated from Cirsium segestum for the first time.
Abstract: Objective To study the chemical constituents of Cirsium segestum. Methods Multi-chromatographic Methods including Silica gel column chromatography and Sephadex LH-20 gel permeation were employed for the isolation and purification.The structures were identified on the basis of chemical evidence and spectral data. Results Five compounds were isolated and identified as Caffeic acid(Ⅰ),Chlorogenic acid(Ⅱ),Baicalin(Ⅲ),stigmasterol 3-O-glucopyranoside(Ⅳ),5,8,4'-trihydroxy-7-O-β-D-glucopyranoside(Ⅴ). Conclusion compounds Ⅳ and Ⅴwere isolated from Cirsium segestum for the first time.
HUANG Xiong-wei, Gu Li-hong. Analyzing the content of rivanol in preparation with back-dropping method[J]. Journal of Pharmaceutical Practice and Service, 2001, (3): 170-171.
Citation:
CAO Qin, CHEN Jian-tao. Studies on the chemical constituents of Cirsium segestum[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(4): 271-273.
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HUANG Xiong-wei, Gu Li-hong. Analyzing the content of rivanol in preparation with back-dropping method[J]. Journal of Pharmaceutical Practice and Service, 2001, (3): 170-171.
HUANG Xiong-wei, Gu Li-hong. Analyzing the content of rivanol in preparation with back-dropping method[J]. Journal of Pharmaceutical Practice and Service, 2001, (3): 170-171.