Message Board

Respected readers, authors and reviewers, you can add comments to this page on any questions about the contribution, review,        editing and publication of this journal. We will give you an answer as soon as possible. Thank you for your support!

Name
E-mail
Phone
Title
Content
Verification Code
x Close Forever Close
Volume 27 Issue 4
. 
Turn off MathJax
Article Contents
Abstract
References
Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2009  >  27(4): 286-288

HUANG Hong-wen, TANG Li-li, TAN Xiao-yong, JIANG Lan-ying. Content determination of hyperoside for Shanzha Maiqu granule by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2009, 27(4): 286-288.
Citation: HUANG Hong-wen, TANG Li-li, TAN Xiao-yong, JIANG Lan-ying. Content determination of hyperoside for Shanzha Maiqu granule by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2009, 27(4): 286-288.
shu

Content determination of hyperoside for Shanzha Maiqu granule by HPLC

  • Shaoguan Institute for Drug Control, Shaoguan 512028, China

  • Received Date: 2008-12-03
  • Objective :To establish a method for determination of hyperoside in Shanzha Maiqu granule. Methods :HPLC was adopted with Agilent ZORBAX SB-C18 column(4.6 mm×250 mm,5 μm),methanol-tetrahydrofuran-0.5% H3PO4(0.917.681.5) as mobile phase at flow rate of 1.0 mL/min and 360 nm as detecting wavelength.Column temperature was room temperature and sample size was 20 μL. Results :The linear range of hyperoside was 0.018 624～0.465 6 μg(r=0.999 9).The average recovery rate of hyperoside was 96.09% and RSD was 0.82%(n=5).The contents of hyperoside in ten batches of Shanzha Maiqu granule were deteminted between 49～65 μg. Conclusion :This method is simple,accurate and reproducible,suitable for quality control of the drug.
  • Created with Highcharts 5.0.7Amount of accessChart context menuAbstract Views, HTML Views, PDF Downloads StatisticsAbstract ViewsHTML ViewsPDF Downloads2024-052024-062024-072024-082024-092024-102024-112024-122025-012025-022025-032025-0400.250.50.7511.25Highcharts.com
    Created with Highcharts 5.0.7Chart context menuAccess Class DistributionFULLTEXT: 81.7 %FULLTEXT: 81.7 %META: 16.9 %META: 16.9 %PDF: 1.4 %PDF: 1.4 %FULLTEXTMETAPDFHighcharts.com
    Created with Highcharts 5.0.7Chart context menuAccess Area Distribution其他: 23.1 %其他: 23.1 %China: 0.6 %China: 0.6 %[]: 0.2 %[]: 0.2 %上海: 1.0 %上海: 1.0 %东莞: 0.8 %东莞: 0.8 %北京: 12.7 %北京: 12.7 %台州: 0.2 %台州: 0.2 %呼和浩特: 0.8 %呼和浩特: 0.8 %哈尔滨: 0.2 %哈尔滨: 0.2 %大连: 0.2 %大连: 0.2 %宁波: 0.2 %宁波: 0.2 %巴音郭楞: 0.2 %巴音郭楞: 0.2 %广州: 0.4 %广州: 0.4 %成都: 0.4 %成都: 0.4 %昆明: 0.6 %昆明: 0.6 %洛阳: 0.4 %洛阳: 0.4 %深圳: 0.8 %深圳: 0.8 %湖州: 0.2 %湖州: 0.2 %潍坊: 1.0 %潍坊: 1.0 %石家庄: 0.2 %石家庄: 0.2 %芒廷维尤: 15.1 %芒廷维尤: 15.1 %衢州: 0.4 %衢州: 0.4 %西宁: 38.6 %西宁: 38.6 %西安: 0.2 %西安: 0.2 %赤峰: 0.2 %赤峰: 0.2 %长沙: 1.4 %长沙: 1.4 %其他China[]上海东莞北京台州呼和浩特哈尔滨大连宁波巴音郭楞广州成都昆明洛阳深圳湖州潍坊石家庄芒廷维尤衢州西宁西安赤峰长沙Highcharts.com
通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索
Get Citation
PDF
XML

Article Metrics

Article views(2861) PDF downloads(918) Cited by()

Related
Proportional views

Content determination of hyperoside for Shanzha Maiqu granule by HPLC

  • Shaoguan Institute for Drug Control, Shaoguan 512028, China
  • Received Date: 2008-12-03

Abstract: Objective :To establish a method for determination of hyperoside in Shanzha Maiqu granule. Methods :HPLC was adopted with Agilent ZORBAX SB-C18 column(4.6 mm×250 mm,5 μm),methanol-tetrahydrofuran-0.5% H3PO4(0.917.681.5) as mobile phase at flow rate of 1.0 mL/min and 360 nm as detecting wavelength.Column temperature was room temperature and sample size was 20 μL. Results :The linear range of hyperoside was 0.018 624～0.465 6 μg(r=0.999 9).The average recovery rate of hyperoside was 96.09% and RSD was 0.82%(n=5).The contents of hyperoside in ten batches of Shanzha Maiqu granule were deteminted between 49～65 μg. Conclusion :This method is simple,accurate and reproducible,suitable for quality control of the drug.

HUANG Hong-wen, TANG Li-li, TAN Xiao-yong, JIANG Lan-ying. Content determination of hyperoside for Shanzha Maiqu granule by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2009, 27(4): 286-288.
Citation: HUANG Hong-wen, TANG Li-li, TAN Xiao-yong, JIANG Lan-ying. Content determination of hyperoside for Shanzha Maiqu granule by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2009, 27(4): 286-288.
shu

    HTML

Catalog

  • HTML

版权所有：《药学实践与服务》编辑委员会

Supervisor & Sponsors: Address: No 325 Guohe Road, ShanghaiPost Code: 200433

Tel: （021）81871324,81871397 E-mail: yxsjzzs@163.com

网站备案号 沪ICP备05003363号-1

Supported by: Beijing Renhe Information Technology Co., Ltd.  

/

DownLoad:  Full-Size Img  PowerPoint
Return
Return