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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2016  >  34(1): 66-71

LE Jiamei, XIONG Xiaojuan, ZHANG Feng, PIAO Shujuan, LU Wenquan. Study on quality standard of Quban oral liquid[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(1): 66-71. doi: 10.3969/j.issn.1006-0111.2016.01.018
Citation: LE Jiamei, XIONG Xiaojuan, ZHANG Feng, PIAO Shujuan, LU Wenquan. Study on quality standard of Quban oral liquid[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(1): 66-71. doi: 10.3969/j.issn.1006-0111.2016.01.018
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Study on quality standard of Quban oral liquid

doi: 10.3969/j.issn.1006-0111.2016.01.018
  • 1.

    Changzheng Hospital, Second Military Medical University, Shanghai 200003, China;College of Chemical and Biological Engineering, Yichun University, Yichun 336000, China

  • 2.

    College of Chemical and Biological Engineering, Yichun University, Yichun 336000, China

  • 3.

    Changzheng Hospital, Second Military Medical University, Shanghai 200003, China

  • Received Date: 2014-11-30
  • Rev Recd Date: 2015-03-17
  • Objective To establish the quality standard for Quban oral liquid. Method Thin layer chromatography(TLC)was used for quality identification of Codonopsis pilosula, Astragalus membranaceus, Paeonia veitchii, Paeonia lactiflora, Atractylodes macrocephala and Angelica sinensis. The paeoniflorin was determined by RP-HPLC. Result Clear spots were obtained with good separation in TLC identification which was highly specific. The paeoniflorin area and content showed a good linear relationship at the range of 18.20-2 330.00 μg/ml (r=0.999 9). The average recovery was 99.72% (RSD=1.25%). Conclusion This method is simple, rapid, accurate, and which can be used for the quality control of Quban oral liquid.
  • [1] 国家药典委员会.中华人民共和国药典2010年版,一部[S].北京:中国医药科技出版社,2010:1282,1050,505,546,606,667,670,683,759,941,967,1050,1178.
    [2] 唐 亮,刘皈阳,李 翔.正骨消肿口服液质量标准研究[J].解放军药学学报,2012,28(5):423-425.
    [3] 彭 洁,许汉香,党安琪,等.血脉舒通口服液质量标准[J].中国医院药学杂志,2004,24(12):781-782.
    [4] 毕晓黎,彭丽诗,李素梅.香芍疏肝口服液质量标准研究[J].江西中医药大学学报,2014,26(2):55-57.
    [5] 张云龙,周迎新.人参养荣口服液质量标准的研究[J].中国药学杂志,1996,31(12):714-716.
    [6] 丁以华,谢升阳,丁 汀.高效液相色谱法测定妇康宝口服液中芍药苷的含量[J].中国医院药学杂志,2007,27(5):697-698.
    [7] 王丽丽,张 宁.高效液相色谱法测定丹芪和肝口服液中芍药苷的含量[J].中国药学杂志,2004,39(1):65.
    [8] 吴绍敏,杨红艳.高效液相色谱法测定赤芍合剂中芍药苷含量[J].中国药业,2011,20(3):20-21.
    [9] 陈 昕,陆兔林,毛春芹.高效液相色谱法测定安心口服液中芍药苷的含量[J].时珍国医国药,2009,20(2):448-449.
    [10] 傅应华,杜 静.反相高效液相色谱法测定健胃灵口服液中芍药苷的含量[J].药物分析杂志.2006,26(11):1671-1673.
    [11] 鲍邢杰,宿树兰.对《中国药典》2010版一部中白芍中芍药苷含量测定方法的探讨[J].时珍国医国药,2012,23(5):1309-1310.
    [12] 焦少珍,韩凤梅,陈 勇.RP-HPLC法同时测定加味逍遥口服液中栀子苷、芍药苷和丹皮酚的含量[J].湖北大学学报(自然科学版),2007,29(2):196-198.
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Study on quality standard of Quban oral liquid

doi: 10.3969/j.issn.1006-0111.2016.01.018
  • 1. Changzheng Hospital, Second Military Medical University, Shanghai 200003, China;College of Chemical and Biological Engineering, Yichun University, Yichun 336000, China
  • 2. College of Chemical and Biological Engineering, Yichun University, Yichun 336000, China
  • 3. Changzheng Hospital, Second Military Medical University, Shanghai 200003, China
  • Received Date: 2014-11-30
  • Rev Recd Date: 2015-03-17

Abstract: Objective To establish the quality standard for Quban oral liquid. Method Thin layer chromatography(TLC)was used for quality identification of Codonopsis pilosula, Astragalus membranaceus, Paeonia veitchii, Paeonia lactiflora, Atractylodes macrocephala and Angelica sinensis. The paeoniflorin was determined by RP-HPLC. Result Clear spots were obtained with good separation in TLC identification which was highly specific. The paeoniflorin area and content showed a good linear relationship at the range of 18.20-2 330.00 μg/ml (r=0.999 9). The average recovery was 99.72% (RSD=1.25%). Conclusion This method is simple, rapid, accurate, and which can be used for the quality control of Quban oral liquid.

LE Jiamei, XIONG Xiaojuan, ZHANG Feng, PIAO Shujuan, LU Wenquan. Study on quality standard of Quban oral liquid[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(1): 66-71. doi: 10.3969/j.issn.1006-0111.2016.01.018
Citation: LE Jiamei, XIONG Xiaojuan, ZHANG Feng, PIAO Shujuan, LU Wenquan. Study on quality standard of Quban oral liquid[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(1): 66-71. doi: 10.3969/j.issn.1006-0111.2016.01.018
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