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Volume 28 Issue 6
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2010  >  28(6): 445-447,474

LI Yue-yue, WANG Hui, CHEN Jun, ZHAO Liang, ZHANG Hai, ZHANG Guo-qing. Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(6): 445-447,474.
Citation: LI Yue-yue, WANG Hui, CHEN Jun, ZHAO Liang, ZHANG Hai, ZHANG Guo-qing. Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(6): 445-447,474.
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Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC

  • Department of Pharmacy,Eastern Hepatobiliary Surgery Hospital,Second Military Medical University,Shanghai,200438,China

  • Received Date: 2010-07-08
  • Rev Recd Date: 2010-09-09
  • Objective To establish a HPLC method for the determination of prim-O-glucosylcimifugin,cimifugin,4'-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhammaudol in Radix Saposhnikoviae. Methods The sample was analyzed on an Agilent Zorbax SB-C18(5 μm,150 mm×4.6 mm id) column with methanol-water mobile phase for the gradient elution.The detection wavelength was 254 nm and flow rate was 0.7 ml/min.The column temperature was 25 ℃ and injection volume was 5 μl. Results The HPLC method for the determination of four major components in Radix Saposhnikoviae was established.The result of method was good. Conclusion The method was simple and feasible,and accurate which could be available for the quality control of Radix Saposhnikoviae.
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    Created with Highcharts 5.0.7Chart context menuAccess Class DistributionFULLTEXT: 83.2 %FULLTEXT: 83.2 %META: 15.8 %META: 15.8 %PDF: 1.0 %PDF: 1.0 %FULLTEXTMETAPDFHighcharts.com
    Created with Highcharts 5.0.7Chart context menuAccess Area Distribution其他: 18.4 %其他: 18.4 %China: 0.3 %China: 0.3 %[]: 0.3 %[]: 0.3 %上海: 2.0 %上海: 2.0 %东莞: 0.3 %东莞: 0.3 %北京: 15.5 %北京: 15.5 %南京: 0.3 %南京: 0.3 %德阳: 0.3 %德阳: 0.3 %杭州: 0.3 %杭州: 0.3 %枣庄: 0.3 %枣庄: 0.3 %芒廷维尤: 5.9 %芒廷维尤: 5.9 %西宁: 54.9 %西宁: 54.9 %西安: 0.3 %西安: 0.3 %鄂州: 0.3 %鄂州: 0.3 %黄山: 0.3 %黄山: 0.3 %其他China[]上海东莞北京南京德阳杭州枣庄芒廷维尤西宁西安鄂州黄山Highcharts.com
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Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC

  • Department of Pharmacy,Eastern Hepatobiliary Surgery Hospital,Second Military Medical University,Shanghai,200438,China
  • Received Date: 2010-07-08
  • Rev Recd Date: 2010-09-09

Abstract: Objective To establish a HPLC method for the determination of prim-O-glucosylcimifugin,cimifugin,4'-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhammaudol in Radix Saposhnikoviae. Methods The sample was analyzed on an Agilent Zorbax SB-C18(5 μm,150 mm×4.6 mm id) column with methanol-water mobile phase for the gradient elution.The detection wavelength was 254 nm and flow rate was 0.7 ml/min.The column temperature was 25 ℃ and injection volume was 5 μl. Results The HPLC method for the determination of four major components in Radix Saposhnikoviae was established.The result of method was good. Conclusion The method was simple and feasible,and accurate which could be available for the quality control of Radix Saposhnikoviae.

LI Yue-yue, WANG Hui, CHEN Jun, ZHAO Liang, ZHANG Hai, ZHANG Guo-qing. Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(6): 445-447,474.
Citation: LI Yue-yue, WANG Hui, CHEN Jun, ZHAO Liang, ZHANG Hai, ZHANG Guo-qing. Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(6): 445-447,474.
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