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Volume 25 Issue 3
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2007  >  (3): 145-146

NI Jin, YE Guang-ming, HU Hong-gang, JIANG Yun-yun, CAI Jian-ming, WU Qiu-ye. Synthesis of methano[6,6]fullerene[C60]carboxylic acid[J]. Journal of Pharmaceutical Practice and Service, 2007, (3): 145-146.
Citation: NI Jin, YE Guang-ming, HU Hong-gang, JIANG Yun-yun, CAI Jian-ming, WU Qiu-ye. Synthesis of methano[6,6]fullerene[C60]carboxylic acid[J]. Journal of Pharmaceutical Practice and Service, 2007, (3): 145-146.
shu

Synthesis of methano[6,6]fullerene[C60]carboxylic acid

  • 1.

    Laboratory of Radiation Medicine, Second Military Medical University, Shanghai 200433, China;

  • 2.

    The 102nd Hospital of PLA, Changzhou 213003, China;

  • 3.

    Department of Organic Chemistry, College of Pharmacy, Second Military Medical University, Shanghai 200433,China

  • Received Date: 2007-03-05
  • Objective:To find good route of synthesizing methano[C60]fullerene carboxylic acid by using bromoactate for preparing some valuable fullerene derivatives.Methods:Using bromoactate as starting material, ylide was prepared. Ylide and fullerene were used to produce the methano[C60] fullerene carboxylate and hydrolyze it.Results and Conclusion: The intermediate and ultimate products synthesized can be confirmed as the objective by NMR and IR, the method is feasible and economical.
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Synthesis of methano[6,6]fullerene[C60]carboxylic acid

  • 1. Laboratory of Radiation Medicine, Second Military Medical University, Shanghai 200433, China;
  • 2. The 102nd Hospital of PLA, Changzhou 213003, China;
  • 3. Department of Organic Chemistry, College of Pharmacy, Second Military Medical University, Shanghai 200433,China
  • Received Date: 2007-03-05

Abstract: Objective:To find good route of synthesizing methano[C60]fullerene carboxylic acid by using bromoactate for preparing some valuable fullerene derivatives.Methods:Using bromoactate as starting material, ylide was prepared. Ylide and fullerene were used to produce the methano[C60] fullerene carboxylate and hydrolyze it.Results and Conclusion: The intermediate and ultimate products synthesized can be confirmed as the objective by NMR and IR, the method is feasible and economical.

NI Jin, YE Guang-ming, HU Hong-gang, JIANG Yun-yun, CAI Jian-ming, WU Qiu-ye. Synthesis of methano[6,6]fullerene[C60]carboxylic acid[J]. Journal of Pharmaceutical Practice and Service, 2007, (3): 145-146.
Citation: NI Jin, YE Guang-ming, HU Hong-gang, JIANG Yun-yun, CAI Jian-ming, WU Qiu-ye. Synthesis of methano[6,6]fullerene[C60]carboxylic acid[J]. Journal of Pharmaceutical Practice and Service, 2007, (3): 145-146.
shu

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