Determination of icarrin in Yangjing capsule by HPLC

LU Xiao-he; JIN Bao-fang; WANG Xiu-lai

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Volume 25 Issue 1

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Article Navigation > Journal of Pharmaceutical Practice and Service > 2007 > (1): 37-38,53

LU Xiao-he, JIN Bao-fang, WANG Xiu-lai. Determination of icarrin in Yangjing capsule by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2007, (1): 37-38,53.

Citation:

LU Xiao-he, JIN Bao-fang, WANG Xiu-lai. Determination of icarrin in Yangjing capsule by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2007, (1): 37-38,53.

Determination of icarrin in Yangjing capsule by HPLC

Nanjing General Hospital of Nanjing Military Command,Nanjing 210002,China

Received Date: 2006-09-18

Abstract

Objective:To establish an HPLC method for determination of Icarrin in Yangjing Capsule. Methods: The determina- tion was performed on Phenomenex C₁₈ column（250mm×4.6 mm,5μm）.The mobile phase consisted of acetonitrile-water（30:70） with a flow rate of 0.8 mL/min.The detecting wavelength was at 270 nm. Results: The linear range of icarrin was 122.2～611.0 ng （r=0.9996）.The average recovery was 98.2%（RSD:1.33% ）. Conclusion: The established method is simple,convenient,accu- rate and reproducible,and suitable for the quality control of Icarrin content in Yangjing capsule.
- Yangjing capsule,
- icarrin,
- HPLC
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

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