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Volume 24 Issue 5
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2006  >  (5): 289-291

HU Jian-guo, LE Jian, LIU Chang-hai, CHEN Gui-Liang. Separation of Enantiomer of Amlodipine by CE and HPLC[J]. Journal of Pharmaceutical Practice and Service, 2006, (5): 289-291.
Citation: HU Jian-guo, LE Jian, LIU Chang-hai, CHEN Gui-Liang. Separation of Enantiomer of Amlodipine by CE and HPLC[J]. Journal of Pharmaceutical Practice and Service, 2006, (5): 289-291.
shu

Separation of Enantiomer of Amlodipine by CE and HPLC

  • Second Chemistry Department of Shanghai drug control institute, Shanghai 200233, China

  • Received Date: 2006-01-15
  • Objective: Separation of enantiomer of amlodipine by CE and HPLC. Methods: Different separation conditions such as buffer pH, the concentration of the chiral selector, buffer concentrations, temperature and applied voltage, etc.were studied and op-timized.The separation was finally conducted in 100mM orthophosphoric acid-Tris buffer (pH3.0) with 1.0% (w/w) HP-β-CD.The applied voltage was 16kV and the temperature 15℃. Results: Both CE and HPLC could give enantiomer of amlodipine resolution for adrenaline. Conclusion: The method proved to be specific and accurate
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    Created with Highcharts 5.0.7Chart context menuAccess Class DistributionFULLTEXT: 87.4 %FULLTEXT: 87.4 %META: 10.4 %META: 10.4 %PDF: 2.3 %PDF: 2.3 %FULLTEXTMETAPDFHighcharts.com
    Created with Highcharts 5.0.7Chart context menuAccess Area Distribution其他: 28.4 %其他: 28.4 %China: 0.9 %China: 0.9 %[]: 0.5 %[]: 0.5 %上海: 2.3 %上海: 2.3 %兰州: 0.5 %兰州: 0.5 %北京: 11.7 %北京: 11.7 %南京: 0.5 %南京: 0.5 %台州: 0.9 %台州: 0.9 %合肥: 0.9 %合肥: 0.9 %杭州: 0.5 %杭州: 0.5 %济宁: 0.5 %济宁: 0.5 %深圳: 0.5 %深圳: 0.5 %湖州: 2.3 %湖州: 2.3 %芒廷维尤: 18.0 %芒廷维尤: 18.0 %西宁: 32.0 %西宁: 32.0 %其他China[]上海兰州北京南京台州合肥杭州济宁深圳湖州芒廷维尤西宁Highcharts.com
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Separation of Enantiomer of Amlodipine by CE and HPLC

  • Second Chemistry Department of Shanghai drug control institute, Shanghai 200233, China
  • Received Date: 2006-01-15

Abstract: Objective: Separation of enantiomer of amlodipine by CE and HPLC. Methods: Different separation conditions such as buffer pH, the concentration of the chiral selector, buffer concentrations, temperature and applied voltage, etc.were studied and op-timized.The separation was finally conducted in 100mM orthophosphoric acid-Tris buffer (pH3.0) with 1.0% (w/w) HP-β-CD.The applied voltage was 16kV and the temperature 15℃. Results: Both CE and HPLC could give enantiomer of amlodipine resolution for adrenaline. Conclusion: The method proved to be specific and accurate

HU Jian-guo, LE Jian, LIU Chang-hai, CHEN Gui-Liang. Separation of Enantiomer of Amlodipine by CE and HPLC[J]. Journal of Pharmaceutical Practice and Service, 2006, (5): 289-291.
Citation: HU Jian-guo, LE Jian, LIU Chang-hai, CHEN Gui-Liang. Separation of Enantiomer of Amlodipine by CE and HPLC[J]. Journal of Pharmaceutical Practice and Service, 2006, (5): 289-291.
shu

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