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Volume 36 Issue 5
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2018  >  36(5): 430-432

YU Jizhi, BAO Jiani, YANG Song. Quality standards of Fufang Huzhangding[J]. Journal of Pharmaceutical Practice and Service, 2018, 36(5): 430-432. doi: 10.3969/j.issn.1006-0111.2018.05.010
Citation: YU Jizhi, BAO Jiani, YANG Song. Quality standards of Fufang Huzhangding[J]. Journal of Pharmaceutical Practice and Service, 2018, 36(5): 430-432. doi: 10.3969/j.issn.1006-0111.2018.05.010
shu

Quality standards of Fufang Huzhangding

doi: 10.3969/j.issn.1006-0111.2018.05.010
  • 1.

    Station for Drug and Instrument Supply, No. 65112 Army Unit of PLA, Shenyang 110026, China

  • 2.

    Institute for Drug and Instrument Control, No. 65112 Army Unit of PLA, Shenyang 110026, China

  • Received Date: 2018-04-27
  • Rev Recd Date: 2018-08-01
  • Objective To establish quality standard for Fufang Huzhangding. Methods Qualitative identification of Polygonum cuspidatum,Apis mellifeta and Borneolum in Fufang Huzhangding by thin layer chromatography;The mobile phase was acetonitrile-water(23:77).The detection wavelength was 306 nm,and the flow rate was 1.0 ml/min.The mobile phase consisted of Agilent Eclipse XDB-C18 column (250 mm×4.6 mm,5 μm), and the column temperature was maintained at 40℃. Results Polygonum cuspidatum,Apis mellifeta and Borneolum in Fufang Huzhangding appeared distinguishing characteristic of TLC,spots were clear,and showed the same reacts with a reference standard.There was a good linear relationship between the concentration of polydatin and the peak area in the range of 8.25-66.0 μg/ml(r=0.999 9).The average recoveries was 100.1%,RSD was 0.2%. Conclusion The method is simple, accurate and reliable, and can be used as a quality control method of the preparation.
  • [1] 国家药典委员会.中华人民共和国药典(一部):2015年版[S].北京:中国医药科技出版社,2015:194-195.
    [2] 田文涛,杨茂文,杨金琰,等.高效液相色谱法测定复方伸筋片中虎杖苷的含量[J].中国药师,2014,17(3):522-523.
    [3] 张国跃,刘春河. RP-HPLC法测定肝康宁片中虎杖苷的含量[J].中国医药科学,2017,7(9):39-41.
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    沈阳化工大学材料科学与工程学院 沈阳 110142

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Quality standards of Fufang Huzhangding

doi: 10.3969/j.issn.1006-0111.2018.05.010
  • 1. Station for Drug and Instrument Supply, No. 65112 Army Unit of PLA, Shenyang 110026, China
  • 2. Institute for Drug and Instrument Control, No. 65112 Army Unit of PLA, Shenyang 110026, China
  • Received Date: 2018-04-27
  • Rev Recd Date: 2018-08-01

Abstract: Objective To establish quality standard for Fufang Huzhangding. Methods Qualitative identification of Polygonum cuspidatum,Apis mellifeta and Borneolum in Fufang Huzhangding by thin layer chromatography;The mobile phase was acetonitrile-water(23:77).The detection wavelength was 306 nm,and the flow rate was 1.0 ml/min.The mobile phase consisted of Agilent Eclipse XDB-C18 column (250 mm×4.6 mm,5 μm), and the column temperature was maintained at 40℃. Results Polygonum cuspidatum,Apis mellifeta and Borneolum in Fufang Huzhangding appeared distinguishing characteristic of TLC,spots were clear,and showed the same reacts with a reference standard.There was a good linear relationship between the concentration of polydatin and the peak area in the range of 8.25-66.0 μg/ml(r=0.999 9).The average recoveries was 100.1%,RSD was 0.2%. Conclusion The method is simple, accurate and reliable, and can be used as a quality control method of the preparation.

YU Jizhi, BAO Jiani, YANG Song. Quality standards of Fufang Huzhangding[J]. Journal of Pharmaceutical Practice and Service, 2018, 36(5): 430-432. doi: 10.3969/j.issn.1006-0111.2018.05.010
Citation: YU Jizhi, BAO Jiani, YANG Song. Quality standards of Fufang Huzhangding[J]. Journal of Pharmaceutical Practice and Service, 2018, 36(5): 430-432. doi: 10.3969/j.issn.1006-0111.2018.05.010
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