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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2017  >  35(4): 355-358

MIAO Jing, TONG Xiaodong. The quality standard research for YI SHI MINGMU granules by HPLC method[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(4): 355-358. doi: 10.3969/j.issn.1006-0111.2017.04.017
Citation: MIAO Jing, TONG Xiaodong. The quality standard research for YI SHI MINGMU granules by HPLC method[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(4): 355-358. doi: 10.3969/j.issn.1006-0111.2017.04.017
shu

The quality standard research for YI SHI MINGMU granules by HPLC method

doi: 10.3969/j.issn.1006-0111.2017.04.017

  • Nantong Hospital of TCM, Nantong 226001, China

  • Received Date: 2016-10-16
  • Rev Recd Date: 2017-01-06
  • Objective To establish the quality standard for YI SHI MINGMU granules. Methods TLC method was used to identify Lycium barbarum L and Salvia miltiorrhiza. HPLC method was used to quantitatively analyze the concentration of Tanshinol sodium. The analysis was carried out on a column of Kromasil C18(4.6 mm×150 mm,5 μm)with a mobile phase of methanol and 0.5 % acetic acid at the flow rate of 0.4 ml/min. Column temperature was 30 ℃. The detection wavelength was 280 nm. Results The linearity range of Tanshinol sodium was 2.00~60.00 μg/ml,r2=0.999 7(n=6),with the average recoveries of 105.62%, RSD=1.60%. Conclusion This method is accurate, simple, reliable and reproducible. It can be used for the quality control of YI SHI MINGMU granules.
  • [1] 汪建龙.枸杞多糖药理作用的研究进展[J]. 时珍国医国药,2005,16(10):1032-1033.
    [2] 郑汉成,蔡少青.药用植物学与生药学[M]. 4版.北京:人民卫生出版社,2004:393.
    [3] 国家药典委员会.中华人民共和国药典2015年版一部[S].北京:中国医药科技出版社,2015:76-77.
    [4] 闫根全.丹参素钠的提取及注射用丹参素钠的研制[D]. 成都:四川大学,2007:6-123.
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The quality standard research for YI SHI MINGMU granules by HPLC method

doi: 10.3969/j.issn.1006-0111.2017.04.017
  • Nantong Hospital of TCM, Nantong 226001, China
  • Received Date: 2016-10-16
  • Rev Recd Date: 2017-01-06

Abstract: Objective To establish the quality standard for YI SHI MINGMU granules. Methods TLC method was used to identify Lycium barbarum L and Salvia miltiorrhiza. HPLC method was used to quantitatively analyze the concentration of Tanshinol sodium. The analysis was carried out on a column of Kromasil C18(4.6 mm×150 mm,5 μm)with a mobile phase of methanol and 0.5 % acetic acid at the flow rate of 0.4 ml/min. Column temperature was 30 ℃. The detection wavelength was 280 nm. Results The linearity range of Tanshinol sodium was 2.00~60.00 μg/ml,r2=0.999 7(n=6),with the average recoveries of 105.62%, RSD=1.60%. Conclusion This method is accurate, simple, reliable and reproducible. It can be used for the quality control of YI SHI MINGMU granules.

MIAO Jing, TONG Xiaodong. The quality standard research for YI SHI MINGMU granules by HPLC method[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(4): 355-358. doi: 10.3969/j.issn.1006-0111.2017.04.017
Citation: MIAO Jing, TONG Xiaodong. The quality standard research for YI SHI MINGMU granules by HPLC method[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(4): 355-358. doi: 10.3969/j.issn.1006-0111.2017.04.017
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