气相色谱-质谱法结合保留指数分析鸭儿芹不同部位挥发油成分

胡思一; 包箐箐; 韩安榜; 向铮; 林崇良

doi:10.3969/j.issn.1006-0111.2015.03.014

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气相色谱-质谱法结合保留指数分析鸭儿芹不同部位挥发油成分

胡思一, 包箐箐, 韩安榜, 向铮, 林崇良

文章导航 > 药学实践与服务 > 2015 > 33(3): 246-249

胡思一, 包箐箐, 韩安榜, 向铮, 林崇良. 气相色谱-质谱法结合保留指数分析鸭儿芹不同部位挥发油成分[J]. 药学实践与服务, 2015, 33(3): 246-249. doi: 10.3969/j.issn.1006-0111.2015.03.014

引用本文:

HU Siyi, BAO Qingqing, HAN Anbang, XIANG Zheng, LIN Chongliang. Volatile components of different parts of Cryptotaenia japonica through GC-MS analysis and Kovats retention index[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(3): 246-249. doi: 10.3969/j.issn.1006-0111.2015.03.014

Citation:

HU Siyi, BAO Qingqing, HAN Anbang, XIANG Zheng, LIN Chongliang. Volatile components of different parts of Cryptotaenia japonica through GC-MS analysis and Kovats retention index[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(3): 246-249. doi: 10.3969/j.issn.1006-0111.2015.03.014

气相色谱-质谱法结合保留指数分析鸭儿芹不同部位挥发油成分

doi: 10.3969/j.issn.1006-0111.2015.03.014

1.
温州医科大学附属第一医院, 浙江温州 325035
2.
温州医科大学药学院, 浙江温州 325035

Volatile components of different parts of Cryptotaenia japonica through GC-MS analysis and Kovats retention index

1.
First Affiliated Hospital of Wenzhou Medical University, Wenzhou 325035, China
2.
Determination Center, Wenzhou Medical University, Wenzhou 325035, China

摘要: 目的研究鸭儿芹不同部位挥发油成分的差异。方法采用水蒸气蒸馏法提取鸭儿芹根、茎、叶、果实中的挥发油,对其进行气相色谱-质谱法(GC-MS)分析,并结合Kovats保留指数对其主要成分进行定性分析。结果鸭儿芹根挥发油检出28个峰,鉴定出28个化合物,占总离子峰的86.66%;鸭儿芹茎挥发油检出27个峰,鉴定出27个化合物,占总离子峰的88.01%;鸭儿芹叶挥发油检出27个峰,鉴定出27个化合物,占总离子峰的94.03%;鸭儿芹果实挥发油检出26个峰,鉴定出26个化合物,占总离子峰的88.32%。鸭儿芹全株共鉴定出35种挥发性化合物,各部位挥发油的主要成分为倍半萜化合物,含有少量的单萜。其中22种化合物为各部位共有,化合物 19 、 23 只存在鸭儿芹根挥发油,香树烯、化合物 25 、红没药醇只存在鸭儿芹果实挥发油,因此它们的种类及相同化合物的含量有一定差异。结论鸭儿芹挥发油含有多种生理活性物质,全草入药有其合理性,为进一步研究开发鸭儿芹提供一定的科学依据。
- 鸭儿芹 /
- 挥发油成分 /
- 气相色谱-质谱法 /
- Kovats保留指数
Abstract: Objective To analyze and compare the chemical components of the volatile oil in different parts of Cryptotaenia japonica. Methods Essential oils were extracted from the root, stem, leaf, fruit of Cryptotaenia japonica through steam distillation. GC-MS analysis combined with Kovats retention index Methods were used to analyze its main components. Results 28 peaks were separated and 28 compounds were identified from volatile oils from the root of Cryptotaenia japonica, accounting for 86.66% of the total, 27 peaks were separated and 27 compounds were identified from volatile oils from stem of Cryptotaenia japonica, accounting for 88.01% of the total, 27 peaks were separated and 27 compounds were identified from volatile oils from leaves of Cryptotaenia japonica, accounting for 94.03% of the total, 26 peaks were separated and 26 compounds were identified from volatile oils from fruit of Cryptotaenia japonica, accounting for 88.32% of the total. 35 kinds of volatile compounds were identified from the whole strain, and the main components of each part of the volatile oil were sesquiterpene compounds, containing a small amount of monoterpenes. Among all the 35 compounds, different parts of Cryptotaenia japonica share 22 compounds. Compounds 19 , 23 only exists in the volatile oil from the roots. Aromadendrene, compound 25 , red myrrh alcohol only exists in the volatile oil from the fruit. So there is a certain difference in the types and quantity of the compounds. Conclusion The volatile oil of Cryptotaenia japonica contains many physiologically active substance. Take the whole plant as a medicine has its rationality, which provide a scientific basis for the further research and development of Cryptotaenia japonica.
- Cryptotaenia japonica /
- volatile oil constituents /
- GC-MS /
- Kovats retention index

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气相色谱-质谱法结合保留指数分析鸭儿芹不同部位挥发油成分

doi: 10.3969/j.issn.1006-0111.2015.03.014

1. 温州医科大学附属第一医院, 浙江温州 325035

2. 温州医科大学药学院, 浙江温州 325035

收稿日期: 2014-02-16
修回日期: 2014-09-10

关键词:

鸭儿芹 /

挥发油成分 /

气相色谱-质谱法 /

Kovats保留指数

摘要: 目的研究鸭儿芹不同部位挥发油成分的差异。方法采用水蒸气蒸馏法提取鸭儿芹根、茎、叶、果实中的挥发油,对其进行气相色谱-质谱法(GC-MS)分析,并结合Kovats保留指数对其主要成分进行定性分析。结果鸭儿芹根挥发油检出28个峰,鉴定出28个化合物,占总离子峰的86.66%;鸭儿芹茎挥发油检出27个峰,鉴定出27个化合物,占总离子峰的88.01%;鸭儿芹叶挥发油检出27个峰,鉴定出27个化合物,占总离子峰的94.03%;鸭儿芹果实挥发油检出26个峰,鉴定出26个化合物,占总离子峰的88.32%。鸭儿芹全株共鉴定出35种挥发性化合物,各部位挥发油的主要成分为倍半萜化合物,含有少量的单萜。其中22种化合物为各部位共有,化合物 19 、 23 只存在鸭儿芹根挥发油,香树烯、化合物 25 、红没药醇只存在鸭儿芹果实挥发油,因此它们的种类及相同化合物的含量有一定差异。结论鸭儿芹挥发油含有多种生理活性物质,全草入药有其合理性,为进一步研究开发鸭儿芹提供一定的科学依据。

English Abstract

Volatile components of different parts of Cryptotaenia japonica through GC-MS analysis and Kovats retention index

1. First Affiliated Hospital of Wenzhou Medical University, Wenzhou 325035, China

2. Determination Center, Wenzhou Medical University, Wenzhou 325035, China

Received Date: 2014-02-16
Rev Recd Date: 2014-09-10

Keywords:

Abstract: Objective To analyze and compare the chemical components of the volatile oil in different parts of Cryptotaenia japonica. Methods Essential oils were extracted from the root, stem, leaf, fruit of Cryptotaenia japonica through steam distillation. GC-MS analysis combined with Kovats retention index Methods were used to analyze its main components. Results 28 peaks were separated and 28 compounds were identified from volatile oils from the root of Cryptotaenia japonica, accounting for 86.66% of the total, 27 peaks were separated and 27 compounds were identified from volatile oils from stem of Cryptotaenia japonica, accounting for 88.01% of the total, 27 peaks were separated and 27 compounds were identified from volatile oils from leaves of Cryptotaenia japonica, accounting for 94.03% of the total, 26 peaks were separated and 26 compounds were identified from volatile oils from fruit of Cryptotaenia japonica, accounting for 88.32% of the total. 35 kinds of volatile compounds were identified from the whole strain, and the main components of each part of the volatile oil were sesquiterpene compounds, containing a small amount of monoterpenes. Among all the 35 compounds, different parts of Cryptotaenia japonica share 22 compounds. Compounds 19 , 23 only exists in the volatile oil from the roots. Aromadendrene, compound 25 , red myrrh alcohol only exists in the volatile oil from the fruit. So there is a certain difference in the types and quantity of the compounds. Conclusion The volatile oil of Cryptotaenia japonica contains many physiologically active substance. Take the whole plant as a medicine has its rationality, which provide a scientific basis for the further research and development of Cryptotaenia japonica.

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气相色谱-质谱法结合保留指数分析鸭儿芹不同部位挥发油成分

doi: 10.3969/j.issn.1006-0111.2015.03.014

Volatile components of different parts of Cryptotaenia japonica through GC-MS analysis and Kovats retention index

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气相色谱-质谱法结合保留指数分析鸭儿芹不同部位挥发油成分

doi: 10.3969/j.issn.1006-0111.2015.03.014

1. 温州医科大学附属第一医院, 浙江 温州 325035 2. 温州医科大学药学院, 浙江 温州 325035

English Abstract

Volatile components of different parts of Cryptotaenia japonica through GC-MS analysis and Kovats retention index

1. First Affiliated Hospital of Wenzhou Medical University, Wenzhou 325035, China 2. Determination Center, Wenzhou Medical University, Wenzhou 325035, China

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目录

1. 温州医科大学附属第一医院, 浙江温州 325035

2. 温州医科大学药学院, 浙江温州 325035

1. First Affiliated Hospital of Wenzhou Medical University, Wenzhou 325035, China

2. Determination Center, Wenzhou Medical University, Wenzhou 325035, China