藏药绵毛丛菔化学成分研究
Study on chemical constituents from Solms-Laubachia lanata
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摘要: 目的 对藏药绵毛丛菔Solms-Laubachia lanata Botsch根部甲醇提取物的化学成分进行分离鉴定。 方法 利用普通硅胶柱色谱方法进行分离、纯化,并经核磁共振(NMR)、质谱(MS)、红外(IR)等现代波谱技术确定其结构。 结果 从绵毛丛菔的甲醇提取物乙酸乙酯部位获得4个化合物,其结构被确定为: β-谷甾醇(Ⅰ),棕榈酸(Ⅱ),胡萝卜苷(Ⅲ),3α ,24-二羟基-齐敦果-12-烯-28-甲酯 (IV)。其中化合物(I)、(III)、(IV)为首次从丛菔属植物中分离得到。Abstract: Objective To isolate and identify the chemical constituents from the root of Solms-Laubachia lanata Botsch. Methods The compounds were isolated by column chromatography. The structures of the were compounds elucidated by spectroscopic analysis (NMR and MS). Results Four compounds were isolated and identified as β-sitosterol, Hexadecontanoic acid, daucosteol, 3α, 24-dihydroxyl-oleanane-12-ene-28-methyl ester. Hexadecontanoic acid, daucosteol, 3α, 24-dihydroxyl-oleanane-12-ene-28-methyl ester were isolated from Solms-Laubachia lanata Botsch for the first time.
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Key words:
- Solms-Laubachia lanata /
- chemical constituents /
- isolation
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[1] 中国植物志编委会. 中国植物志[M]. 北京: 科学出版社, 1979, 33: 330. [2] 胡幼华. 宽果丛菔化学成分的研究[J]. 哈尔滨师范大学自然科学学报, 1995,11(2): 71. [3] 倪志诚, 李乾振, 周榜弟, 等. 西藏经济植物[M]. 北京:科学技术出版社,1990: 248. [4] 巨 勇, 贾忠建, 朱子清. 九节菖蒲化学成分研究[J]. 中草药, 1986, 17(9): 4. [5] 从蒲珠, 苏克曼. 分析化学手册.质谱分册[M].第2版.北京: 化学工业出版社,2000:294. [6] Rogelio PM, Guiliermo D, Alfonso RDV. New triterpenoids from Salvia Nicolsonia[J]. Journal of Natural Products, 1986, 49(2): 225. -
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